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Synthesis of magnetite hydrosols in inert atmosphere

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Abstract

A setup is described for magnetite hydrosol synthesis in inert atmosphere via coprecipitation of bi- and trivalent iron salts in the presence of a base with the formation of nanoparticles having desired sizes and chemical composition. The size of nanoparticles is estimated based on analysis of light-scattering and transmission-electron-microscopy data. The chemical composition of magnetite nanoparticles is monitored by Raman spectroscopy.

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References

  1. Yu, D.B., Sun, X.Q., Zou, J.W., Wang, Z.R., Wang, F., and Tang, K., J. Phys. Chem. B, 2006, vol. 110, p. 21667.

    Article  CAS  Google Scholar 

  2. Arruebo, M., Galan, M., Navascues, N., Tellez, C., Marquina, C., Ibarra, M.R., and Santamaria, J., J. Chem. Mater., 1911, p. 18.

    Google Scholar 

  3. Correa-Duarte, M.A., Giersig, M., Kotov, N.A., and Liz-Marzan, L.M., Langmuir, 1998, vol. 14, p. 6430.

    Article  CAS  Google Scholar 

  4. Mamedov, A.A. and Kotov, N., Langmuir, 2000, vol. 16, p. 5530.

    Article  CAS  Google Scholar 

  5. Zhang, D. and Fakhrullin, R.F., Ozmen, M., Wang, H., Wang, J., Paunov, V.N., Li, G., and Huang, W.E., Microb. Biotechnol., 2011, vol. 4, p. 89.

    Article  CAS  Google Scholar 

  6. Fang, M., Grant, P.S., McShane, M.J., Sukhorukov, G.B., Golub, V.O., and Lvov, Y.M., Langmuir, 2002, vol. 18, p. 6338.

    Article  CAS  Google Scholar 

  7. Kolesnikova, T.A., Akchurin, Ga.G., Portnov, S.A., Khomutov, G.B., Akchurin, Ge.G., Naumova, O.G., Sukhorukov, G.B., and Gorin, D.A., Laser Phys. Lett., 2012, vol. 9, p. 643.

    CAS  Google Scholar 

  8. Shchukin, D.G., Gorin, D.A., and Mohwald, H., Langmuir, 2006, vol. 22, p. 7400.

    Article  CAS  Google Scholar 

  9. Andreeva, D.V., Gorin, D.A., Shchukin, D.G., and Sukhorukov, G.B., Macromol. Rapid Commun., 2006, vol. 27, p. 931.

    Article  CAS  Google Scholar 

  10. Grigoriev, D., Gorin, D., Sukhorukov, G.B., Yashchenok, A., Maltseva, E., and Mohwald, H., Langmuir, 2007, vol. 23, p. 12388.

    Article  CAS  Google Scholar 

  11. Dincer, I., Tozkoparan, O., German, S.V., Markin, A.V., Yildirim, O., Khomutov, G.B., Gorin, D.A., Venig, S.B., and Elerman, Y., J. Magn. Magn. Mater., 2012, vol. 324, p. 2958.

    Article  CAS  Google Scholar 

  12. Yashchenok, A.M., Gorin, D.A., Badylevich, M., Serdobintsev, A.A., Bedard, M., Fedorenko, Y.G., Khomutov, G.B., Grigoriev, D.O., and Mohwald, H., Phys. Chem. Chem. Phys., 2010, vol. 12, p. 10469.

    Article  CAS  Google Scholar 

  13. Kolasinska, M., Gutberlet, T., and Krastev, R., Langmuir, 2009, vol. 25, p. 10292.

    Article  CAS  Google Scholar 

  14. Chin, A.B. and Yaacob, I.I., J. Mater. Process. Technol., 2007, vol. 191, p. 235.

    Article  CAS  Google Scholar 

  15. Albornoz, C. and Jacobo, S.E., J. Magn. Magn. Mater., 2006, vol. 305, p. 12.

    Article  CAS  Google Scholar 

  16. Kim, E.H., Lee, H.S., Kwak, B.K., and Kim, B.K., J. Magn. Magn. Mater., 2005, vol. 289, p. 328.

    Article  CAS  Google Scholar 

  17. Wan, J., Chen, X., Wang, Z., Yang, X., and Qian, Y., J. Cryst. Growth, 2005, vol. 276, p. 571.

    Article  CAS  Google Scholar 

  18. Kimata, M., Nakagawa, D., and Hasegawa, M., Powder Technol., 2003, vol. 132, p. 112.

    Article  CAS  Google Scholar 

  19. Massart, R., IEEE Trans. Magn., 1981, vol. 17, p. 1247.

    Article  Google Scholar 

  20. Taketomi, S. and Chikazumi, S., Magnetic Fluids, Tokyo: Nikkan, 1988.

    Google Scholar 

  21. Martinez-Mera, I., Espinosa, M.E., Perez-Hernandez, R., and Arenas-Alatorre, J., Mater. Lett., 2007, vol. 61, p. 4447.

    Article  CAS  Google Scholar 

  22. Morrison, S.A., Cahill, C.L., Carpenter, E., Calvin, S., and Harris, V.G., J. Nanosci. Nanotechnol., 2005, vol. 5, p. 1323.

    Article  CAS  Google Scholar 

  23. Sun, Y.-K., Ma, M., Zhang, Y., and Gu, N., Colloids Surf. A, 2004, vol. 245, p. 15.

    Article  CAS  Google Scholar 

  24. Qiu, J., Yang, R., Li, M., and Jiang, N., Mater. Res. Bull., 2005, vol. 40, p. 1968.

    Article  CAS  Google Scholar 

  25. Lee, S.-J., Jeong, J.-R., Shin, S.-C., Kim, J.-C., and Kim, J.-D., J. Magn. Magn. Mater., 2004, vol. 282, p. 147.

    Article  CAS  Google Scholar 

  26. http://rsb.info.nih.gov/ij/

  27. Gupta, A.K. and Curtis, A.S.G., Biomaterials, 2004, vol. 25, p. 3029.

    Article  CAS  Google Scholar 

  28. Gupta, A.K. and Gupta, M., Biomaterials, 2005, vol. 26, p. 3995.

    Article  CAS  Google Scholar 

  29. Sjogren, C.E., Briley-Saebo, K., Hanson, M., and Johansson, C., Magn. Reson. Med., 1994, vol. 31, p. 268.

    Article  CAS  Google Scholar 

  30. Cornell, R.M. and Schertmann, U., Iron Oxides in the Laboratory: Preparation and Characterization, Weinheim: VCH, 1991.

    Google Scholar 

  31. Cotton, F.A. and Wilkinson, G., Advanced Inorganic Chemistry, New York: Wiley, 1988.

    Google Scholar 

  32. Shebanova, O.N. and Lazor, P., J. Raman Spectrosc., 2003, vol. 34, p. 845.

    Article  CAS  Google Scholar 

  33. Jubb, A.M. and Allen, H.C., ACS Appl. Mater. Interfaces, 2010, vol. 2, p. 2804.

    Article  CAS  Google Scholar 

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Authors and Affiliations

  1. Chernyshevskii Saratov State University, Astrakhanskaya ul. 83, Saratov, 410012, Russia

    S. V. German, O. A. Inozemtseva, A. V. Markin, Kh. Metvalli & D. A. Gorin

  2. Moscow State University, Moscow, 119899, Russia

    G. B. Khomutov

Authors
  1. S. V. German
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  2. O. A. Inozemtseva
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  3. A. V. Markin
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  4. Kh. Metvalli
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  5. G. B. Khomutov
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  6. D. A. Gorin
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Additional information

Original Russian Text © S.V. German, O.A. Inozemtseva, A.V. Markin, Kh. Metvalli, G.B. Khomutov, D.A. Gorin, 2013, published in Kolloidnyi Zhurnal, 2013, Vol. 75, No. 4, pp. 534–537.

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German, S.V., Inozemtseva, O.A., Markin, A.V. et al. Synthesis of magnetite hydrosols in inert atmosphere. Colloid J 75, 483–486 (2013). https://doi.org/10.1134/S1061933X13040042

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  • DOI: https://doi.org/10.1134/S1061933X13040042

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