Acylation of 3,4-dihydro-1-methylisoquinoline with substituted acryloyl chlorides followed by irradiation of the resulting enamides provides a useful synthetic route to the benzo[a]quinolizines (4), (8a–d), and (9a) and (9b), and has been applied to a new total synthesis of flavopereirine (14).
I. Ninomiya, Y. Tada, T. Kiguchi, O. Yamamoto and T. Naito, J. Chem. Soc., Perkin Trans. 1, 1984, 2035 DOI: 10.1039/P19840002035
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