SCHEDULED MAINTENANCE
The reaction of thiols with N2O4 in an inert organic solvent such as CCl4 or ether at low temperatures afforded aryl and alkyl thionitrites in quantitative yields; the thionitrites thus obtained reacted very readily with other thiols or sulphinic acids to give unsymmetrical disulphides or thiolsulphonates in nearly quantitative yields.
S. Oae, D. Fukushima and Y. H. Kim, J. Chem. Soc., Chem. Commun., 1977, 407b DOI: 10.1039/C3977000407B
To request permission to reproduce material from this article, please go to the Copyright Clearance Center request page.
If you are an author contributing to an RSC publication, you do not need to request permission provided correct acknowledgement is given.
If you are the author of this article, you do not need to request permission to reproduce figures and diagrams provided correct acknowledgement is given. If you want to reproduce the whole article in a third-party publication (excluding your thesis/dissertation for which permission is not required) please go to the Copyright Clearance Center request page.
Read more about how to correctly acknowledge RSC content.
Please wait while we load your content...