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Characterization of Nanoparticles by Scattering Techniques

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Abstract

Basic principles and applications of different scattering techniques (including static and dynamic light scattering (SLS and DLS), small-angle X-ray scattering (SAXS), wide-angle X-ray diffraction (WAXD) and small-angle neutron scattering (SANS)) on the characterization of nanoparticles are reviewed in this paper. By choosing a suitable scattering technique or a combination of different techniques for nanoparticle characterization, the particles' molecular weight, radius of gyration, hydrodynamic radius, size distribution, shape and internal structure as well as interparticle interactions of nanoparticles, can be determined. Examples including some sophisticated colloidal systems are presented.

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References

  1. Chu B., 1991. Laser Light Scattering, 2nd edn. Academic Press, New York.

    Google Scholar 

  2. Berne B.J. and Pecora R., 1976. Dynamic Light Scattering, John-Wiley & Sons, New York.

    Google Scholar 

  3. Schmitz K.S. 1990. An Introduction to Dynamic Light Scattering by Macromolecules. Academic Press, San Diego.

    Google Scholar 

  4. Brown W., ed., 1993. Dynamic Light Scattering: The methods and Some Applications. Clarendon Press, Oxford.

    Google Scholar 

  5. Chu B., 1995. Quasi-Elastic Light Scattering. In: Richards R.W., ed., Scattering Methods in Polymer Science., Ellis Horwood Ltd., Great Britain, pp. 6-25.

    Google Scholar 

  6. Chu B., 1993. J. Polymer Sci., Polym. Phys. Ed. 31, 2019.

    Google Scholar 

  7. Chu B. and Zhou, Z., 1993, Scattering techniques applied to food systems: light scattering and small angle X-ray scattering. In: Baianu I.C., Pessen H. and Kumosinski T.F., eds., New Techniques and Applications of Physical Chemistry to Food Systems (Physical Chemistry of Food Processes, Vol. II, 245). Van Nostrand Reinhold, New York.

    Google Scholar 

  8. Wu C. and Chu, B., 1998. Light scattering. In: Tanaka T., Grosberg A. and Doi M., eds., Handbook of Polymer Sciences: Experimental Methods in Polymer Science. Modern Methods in Polymer Research and Technology. Academic Press, Boston, MA.

    Google Scholar 

  9. Booth C. and Price C., eds. 1989. Comprehensive Polymer Science: The Synthesis, Characterization, Reactions and Applications of Polymers. Pergamon Press, Oxford, England; Vol.1.

    Google Scholar 

  10. Provencher S.W., 1976. Biophys. J. 16, 29.

    Google Scholar 

  11. Provencher S.W., 1976. J. Chem. Phys. 64(7), 2772.

    Google Scholar 

  12. Nyeo S.-L. and Chu, B., 1989. Macromolecules 22(10), 3998.

    Google Scholar 

  13. Sun C.D., Wang Z., Wu G., and Chu B. 1992. Macromolecules 25(3), 1114.

    Google Scholar 

  14. Wu, D.Q., Chu, B., Lundberg R.D. and MacKnight, W.J., 1993. Macromolecules 26, 1000.

    Google Scholar 

  15. Glatter O. and Kratky O., 1982. Small Angle X-Ray Scattering. Academic press, London.

    Google Scholar 

  16. Yang Y.-W., Yang Z., Zhou Z., Attwood D. and Booth C., 1996. Macromolecules 29, 670.

    Google Scholar 

  17. Zhou S.,Wan Q., Liang D., Chu B., Xu P. and Lai J. J. Appl. Polym. Sci. (in press).

  18. Liu T., Zhou Z., Wu C., Chu B., Schneider D.K. and Nace V.M., 1997. J. Phys. Chem. B. 101, 8808.

    Google Scholar 

  19. Cullity B.D., 1978. Elements of X-ray Diffraction, 2nd edn. Addison-Wesley Publishing Company Inc., MA, USA.

    Google Scholar 

  20. Wu C., Liu T., Chu B., Schneider D.K. and Graziano V., 1997. Macromolecules 30, 4574.

    Google Scholar 

  21. Alexandridis P., Olsson U. and Lindman B., 1995. Macromolecules 28, 7700.

    Google Scholar 

  22. Alexandridis P., Olsson U. and Lindman B., 1998. Langmuir 14, 2627.

    Google Scholar 

  23. Wu G., Zhou Z. and Chu B., 1993. J. Polym. Sci., Part B: Polym. Phys. 31, 2035.

    Google Scholar 

  24. Chu B., 1995. Langmuir 11, 414.

    Google Scholar 

  25. Dobeshi T., Narita T., Masuda J., Makino K., Mogi T., Ohshima H., Takenata M. and Chu B., 1998. Langmuir 14, 748.

    Google Scholar 

  26. Dresco P.A., Zaitsev V.S., Gambino R.J. and Chu B., 1999. Langmuir 15, 1945.

    Google Scholar 

  27. Chemical Reviews (1999) 99, the reviews and references therein.

  28. DeSimone J.M., Maury E.E., Menceloglu Y.Z., McClain J.B., Romack T.R. and Combes J.R., 1994. Science 265, 356.

    Google Scholar 

  29. Ji M., Chen X., Wai C.M. and Fulton J.L., 1999. J. Am. Chem. Soc. 121, 2631.

    Google Scholar 

  30. Zhou S., Chu B. and Dhadwal H.S., 1998, Rev. Sci. Insrum. 69(5), 1955.

    Google Scholar 

  31. Zhou S. and Chu B., 1998. Macromolecules 31, 5300.

    Google Scholar 

  32. Zhou S. and Chu B., 1998. Macromolecules 31, 7746.

    Google Scholar 

  33. Liu L.-Z., Cheng Z., Inomata K., Zhou S. and Chu B., 1999. Macromolecules 32, 5836.

    Google Scholar 

  34. Zero K. and Pecora R., 1985. Dynamic depolarized light scattering In: Pecora R., ed., Dynamic Light Scattering: Applications of Photon Correlation Spectroscopy. Plenum Press, New York.

    Google Scholar 

  35. Tolstoi N.A. and Feofilov P.P., 1949. Dokl. Akad. Nauk SSSR, 66, 617.

    Google Scholar 

  36. Benoit H., 1949. Compt. Rend. 228, 1716.

    Google Scholar 

  37. O'Konski C.T. and Zimm B.H., 1950. Science 111, 113.

    PubMed  Google Scholar 

  38. Munk P. 1989. Introduction to Macromolecular Science. John-Wiley & Sons: New York.

    Google Scholar 

  39. Zhou S., Fan S., Au-Yeung S.C.F. and Wu C., 1995. Polymer, 36(7), 1341.

    Google Scholar 

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Chu, B., Liu, T. Characterization of Nanoparticles by Scattering Techniques. Journal of Nanoparticle Research 2, 29–41 (2000). https://doi.org/10.1023/A:1010001822699

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