Chemoenzymatic Synthesis of Optically Active 2-Phenyl-2-(1H-1,2,4-triazol-1-ylmethyl)hexanenitrile
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General
1H NMR (250 or 300 MHz) and 13C NMR spectra (63 or 75 MHz) were recorded on a Varian Gemini 250 or 300 MHz spectrometer with TMS as an internal reference. IR spectra were recorded on a MIDAC 101025 FT-IR spectrometer and optical rotation was measured on Autopol® III polarimeter (Rudolph Research Co.). Low EI resolution mass spectra were determined on HP GC 5972 [Column: Hewlett-Packard fused silica capillary column HP-5 cross-linked 5% Phenyl methyl silicone, Column ID 0.20 mm, Film thickness: 0.11
Acknowledgements
We are grateful to the Korea Institute of Science and Technology for financial support and Dr Kwan Mook Kim for X-ray crystallographic analysis.
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