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Synthesis and characterization of magnetic porous clay heterostructure

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Abstract

Magnetic porous clay heterostructure (magnetic PCH) was successfully synthesized using a simple precipitation method of applying magnetite onto a PCH surface. X-ray techniques were used to confirm the presence of magnetite in the composite. The magnetite particles, as investigated by the transmission electron microscopy, were spherical nanoparticles (~12.07 nm). The magnetic PCH exhibited characteristics of mesoporous material type IV, similar to PCH. Significant enhancement of the magnetic and dielectric properties in the high frequency range was also observed.

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Acknowledgments

The authors would like to acknowledge the receipt of a research grant from the National Research Council of Thailand (NRCT), and partial support from the 90th Anniversary of Chulalongkorn University Fund (Ratchadaphiseksomphot Endowment Fund). Additionally, the authors are thankful for the use of the experimental facilities at the Polymer Processing and Polymer Nanomaterials Research Unit of the Petroleum and Petrochemical College, Chulalongkorn University. We sincerely appreciate to Asst. Prof. Dr. Pongsakorn Jantaratana, Department of Physics, Kasetsart University, for his kind assistance with the Vibration Sample Magnetometer measurement. Finally, NB would like to acknowledge his PhD scholarship from the Thailand Graduate Institute of Science and Technology (TGIST).

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Authors and Affiliations

  1. The Petroleum and Petrochemical College, Chulalongkorn University, Bangkok, 10330, Thailand

    Natthaphon Bunnak, Sarute Ummartyotin & Hathaikarn Manuspiya

  2. National Metal and Materials Technology Center, Pathumthani, 12120, Thailand

    Pitak Laoratanakul

  3. Department of Electrical and Computer Engineering, College of Engineering, The University of Texas at San Antonio, San Antonio, TX, 78249, USA

    Amar S. Bhalla

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  1. Natthaphon Bunnak
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  2. Sarute Ummartyotin
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  3. Pitak Laoratanakul
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  4. Amar S. Bhalla
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  5. Hathaikarn Manuspiya
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Correspondence to Hathaikarn Manuspiya.

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Bunnak, N., Ummartyotin, S., Laoratanakul, P. et al. Synthesis and characterization of magnetic porous clay heterostructure. J Porous Mater 21, 1–8 (2014). https://doi.org/10.1007/s10934-013-9739-6

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