A technique for quantitative analysis of 3-aminopropylsilane on the surface of chemically modified Fe3O4 magnetic nanoparticles in the concentration range 0.32–3.03 mmol/g was developed using attenuated total reflection infrared spectroscopy. The technique was based on the ratios of band areas corresponding to Fe–O vibrations of the nanoparticles and Si–O vibrations of the coating as a function of the Si mass fraction in the nanocomposite that was determined by inductively coupled plasma atomic-emission spectroscopy.
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Translated from Zhurnal Prikladnoi Spektroskopii, Vol. 81, No. 4, pp. 510–514, July–August, 2014.
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Demin, A.M., Koryakova, O.V. & Krasnov, V.P. Quantitative Determination of 3-Aminopropylsilane on the Surface of FE3O4 Nanoparticles by Attenuated Total Reflection Infrared Spectroscopy. J Appl Spectrosc 81, 565–569 (2014). https://doi.org/10.1007/s10812-014-9970-1
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DOI: https://doi.org/10.1007/s10812-014-9970-1